PROCESS FOR THE PURIFICATION OF CRUDE PROPENE OXIDE
Application 1240/KOLNP/2005 published 2006-06-23, filed 2005-06-28
The present invention relates to a process for the purification of a crude propene oxide containing methanol and acetaldehyde by a continuously operated extractive distillation using an extraction solvent lowering the volatility of methanol and feeding a compound containing an unsubstituted NH2 group capable of reacting with acetaldehyde to a distillation column at a point above the feeding point of the crude propene oxide to give a purified propene oxide containing less than 100 ppm methanol and less than 100 ppm acetaldehyde. The invention also relates to a process for the catalytic epoxidation of propene that includes this purification stage. (FIG. - Nil)
Applicant
DEGUSSA AG & UHDE GMBH
BENNIGSENPLATZ 1, DE-40474 DUSSELDORF GERMANY & FRIEDRICH-UHDE-STRASSE 15 DE 44141 DORTMUND GERMANY
Inventor
WILLI HOFEN SUDRING THOMAS HAAS WOLFGANG WOLL GEORG THIELE
International Info
Classification: C07D 301/32
Publication Number: WO 04/048355 A1
Application Date: 2003-11-25
Priority Information
02026240.8 EP 2002-11-26